Modular Sampling System Initiative Background and Status 2000 Fall Sponsor Meeting Center for Process Analytical Chemistry Modular Sampling System Initiative CPAC: Nov 6, 2000
Agenda • Status and Update • Preview of Swagelok Proposal Modular Sampling System Initiative CPAC: Nov 6, 2000
CPAC as a Multi-Purpose PA Forum • Legal Umbrella for Sponsors to Meet R&D: Long Range / Short Range Information Clearing House Enabling Mechanism to Address Other Common Needs • Focus Groups: Forum to Review R&D Programs Present Industry Common Needs - RFP Address Industry Common Needs Fieldbus Datalink Specification - Done Ne. SSI - In progress Mat. Lab On-line/Connectivity - Future? Modular Sampling System Initiative CPAC: Nov 6, 2000
Background and Chronology of Ne. SSI Activities • O&P Focus Group May 1999 Identified Sampling Systems as Common Area Of Interest Sponsored Tutorial for Nov 99 Sponsor Meeting • Tutorial Nov 99 CPAC Meeting Background/Reasons for Interest Presentations by Suppliers/ End Users • Participation in IFPAC 2000 Meeting Plenary/General Papers (SS Enjoyed High Profile) Workshop Modular Sampling System Initiative CPAC: Nov 6, 2000
Sampling System Vision FLAN (Optical Fiber) Sensor = Moisture Probe P T F A IA Control ler (ASIC) Sensor/Signal Bus Modular Sampling System Initiative CPAC: Nov 6, 2000
Process Analyzer Vision Modular Sampling System Initiative CPAC: Nov 6, 2000
Background and Chronology of Ne. SSI Activities (cnt’d) • Ad-hoc O&P Meeting @ Pittcon 2000 End-users Discuss Initial Target Designs • CPAC 2000 Spring Meeting Formed SS Focus Group Defined Information Package (basis of RFP) • Distributed RFP (July 2000) Clarification Meeting at ISAEXPO 2000 (40 attendees) Received Proposals from Swagelok, Parker Expect Additional Proposals/Comments from Autoflow, ABB Analytical, SAAI, Rosemount Analytical Modular Sampling System Initiative CPAC: Nov 6, 2000
Background and Chronology of Ne. SSI Activities (cnt’d) • CPAC 2000 Fall Meeting Preview of Swagelok Proposal Other Feedback Micro-Reactor Proposal (Micro. Analytics) • What is Next? Distribute Proposals to All Interested Parties Follow-up by Report Sampling System Session at IFPAC 2001 Review and Summary of Ne. SSI Effort Papers by Swagelok, Parker, Autoflow, ABB, Rosemount Modular Sampling System Initiative CPAC: Nov 6, 2000
Acknowledgements • Dow Rob Dubois/Ron O’Reily/ Brian Worthington • Dow Corning Jim Tatera/Gary Bokerman • Du. Pont Bob Bucher • Rohm&Haas Joe Sung • Honeywell Ken Creasy • Akzo Nobel Foad Mozayeni • Exxon. Mobil Dan Podkulski/Rajko Puzic/ John Cumbus/Jeff Gunnell • Swagelok Dave Simko • CPAC Lloyd Burgess/Larry Ricker Modular Sampling System Initiative CPAC: Nov 6, 2000
The End Modular Sampling System Initiative CPAC: Nov 6, 2000
O&P Focus Group Meeting May 99 • Recognized Modular Sampling System Efforts in Semi Conductor Industry (Standard) • Vendors like Autoflow, A+, Swagelok etc. promoted modular designs • Recognized that current implementations of sample systems designs have not changed for many years • CPAC has promoted Versatile Micro Analytical Systems (VMAS) as a basis for future micro-analytical techniques • O&P decided to sponsor a SSISSS (Small Smart Integrated Sensor and Sampling System) Tutorial at CPAC Nov Meeting Modular Sampling System Initiative CPAC: Nov 6, 2000
Nov 99 CPAC SSISSS Tutorial • Exxon. Mobil/Du. Pont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System • Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) • Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers Modular Sampling System Initiative CPAC: Nov 6, 2000
Driving Forces for Change • Reduce Cost of Ownership Non Recurring Costs = Cost to Build Operating Cost • Data Validation (Fit for Use) Modular Sampling System Initiative CPAC: Nov 6, 2000
Integration of Sample System and Sensors All System Components in Contact with Sample including the Sensors Modular Sampling System Initiative Sample Conditioning System Process Stream Field LAN A Mainly a Trust Configuration Now a Trust & Verify Configuration P T F Level 0 Analyzer Controller All Additional Electronic and Computing Components Required to Generate Analytical Result Level 1 CPAC: Nov 6, 2000
Level 0 Subsystem Integration Purpose: Prepare and Verify a Representative Sample (Compatible with Analyzer Sensor) Sample Conditioning System Integrated Sampling/Sensor System Process Stream A P Opportunity: T • Size • Cost F Packaging as an Integrated Sensor and Sampling System Issues: Standardization • Level 0 Size • Modular Sampling System Initiative • VMAS CPAC: Nov 6, 2000
Separation or Integration of Level 0/1 Subsystems Objective: Close to Sample Tap Field LAN Integrated Sampling/Sensor System Process Stream A P T F Analyzer Controller Options: • Remote • Separate but Close • Integrated Modular Sampling System Initiative Level 0 Level 1 CPAC: Nov 6, 2000
Integration of Level 0/1 Subsystems Integrated Sampling/Sensor/Controller System Process Stream Field LAN A P $$ T Analyzer Controller F Modular Sampling System Initiative Level 0 Level 1 CPAC: Nov 6, 2000
Nov 99 CPAC SSISSS Tutorial • Exxon. Mobil/Du. Pont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System • Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) • Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers Modular Sampling System Initiative CPAC: Nov 6, 2000
Nov 99 CPAC SSISSS Tutorial (Vendor Presentations) Swagelok Autoflow A+ Modular Sampling System Initiative Rosemount CPAC: Nov 6, 2000
Nov 99 CPAC SSISSS Tutorial • Exxon. Mobil/Du. Pont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System • Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) • Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) and Micro Fluidics Sensors/Analyzers Modular Sampling System Initiative CPAC: Nov 6, 2000
IFPAC 2000 • Exxon. Mobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design for SSISSS Highlighted sensor and analyzer transmitter configurations • Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile • CPAC/Exxon. Mobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort Modular Sampling System Initiative CPAC: Nov 6, 2000
TODAY’S COST OF BUILD For a major greenfield project Modular Sampling System Initiative CPAC: Nov 6, 2000
TODAY’S COST OF OWNERSHIP Modular Sampling System Initiative CPAC: Nov 6, 2000
IMAGINE THE FUTURE P T Analyzer Controller F Level 0 Modular Sampling System Initiative Field LAN Process Stream A Level 1 CPAC: Nov 6, 2000
IMAGINE THE FUTURE FLAN (Optical Fiber) Sensor = Moisture Probe P T F A IA Controller (ASIC) & Interface Module Sensor/Signal Bus Original Picture of Gas Delivery System courtesy Valin Corporation; Modular Sampling System Initiative CPAC: Nov 6, 2000
IMAGINE THE FUTURE Sensor = RAMAN Probe P T F Interface Module A Modular Sampling System Initiative CPAC: Nov 6, 2000
IFPAC 2000 • Exxon. Mobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design fro SSISSS Highlighted sensor and analyzer transmitter configurations • Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile • CPAC/Exxon. Mobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort Modular Sampling System Initiative CPAC: Nov 6, 2000
IFPAC 2000 • Exxon. Mobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design fro SSISSS Highlighted sensor and analyzer transmitter configurations • Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile • CPAC/Exxon. Mobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort Modular Sampling System Initiative CPAC: Nov 6, 2000
Pittcon 2000 (New Orleans) • O&P Ad-Hoc Meeting of Sponsor End-users Du. Pont, Dow-Corning, CPAC, Rohm&Haas, Exxon. Mobil • Main Goal: Identify Typical Sample System Designs as Candidates for Modular Design Reviewed some typical gas/liquid sample System Designs Rob Du. Bois Presented a Modular Component/Service Matrix • Discussed next steps Present Sample System Data at May CPAC Meeting Next Step is to Open Up Discussion (3 rd parties) Leverage ISA Meeting in New Orleans (Aug 00) • Role of CPAC in Facilitating Development/Testing of a Prototype System Larry Ricker/Lloyd Burgess to Present Proposal Modular Sampling System Initiative CPAC: Nov 6, 2000
Status • CPAC Meeting May 1999 Done O&P Identified Modular Sampling Systems • CPAC Meeting Nov 1999 Done O&P Sponsored Tutorial • IFPAC 2000 Meeting Done Plenary Presentation Promoted SSISS Session on Modular Sampling Systems CPAC Sponsored Workshop • Pittcon 2000 Done Ad-hoc O&P Meeting Propose Candidate Sampling System Descriptions • CPAC Meeting May 2000 Modular Sampling System Initiative TBD CPAC: Nov 6, 2000
What is Next? • CPAC Meeting May 2000 (Sampling Focus Group – Wednesday) Review and Agree on Sample System Information Package Involvement of 3 rd parties How do we distribute package (Distribution List, Meeting? ) Expectations for proposals from Suppliers (Paper designs? ) Joint Effort with ISA (Meeting in Aug, New Orleans) Evaluation of Designs - Recommendation • Prototype design/manufacturing/testing at CPAC Larry Ricker/Lloyd Burgess proposal • Program to Evaluate Test Platforms fro Micro Analytical Devices CPAC Proposal – Lloyd Burgess Modular Sampling System Initiative CPAC: Nov 6, 2000
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