Скачать презентацию Kappa Workgroup Meeting September 20 -21 2009 EMBL Скачать презентацию Kappa Workgroup Meeting September 20 -21 2009 EMBL

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Kappa Workgroup Meeting September 20 -21, 2009 EMBL Grenoble Staus Report EMBL Hamburg Gleb Kappa Workgroup Meeting September 20 -21, 2009 EMBL Grenoble Staus Report EMBL Hamburg Gleb Bourenkov

EMBL@Petra. III 20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup [email protected] III 20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup

MX 1 Michele Cianci MX 2 Gleb Bourenkov Bio. SAXS Manfred Roessle Energy [ke. MX 1 Michele Cianci MX 2 Gleb Bourenkov Bio. SAXS Manfred Roessle Energy [ke. V] 5(4)-17 7 -35 4 -20 Monochromators Si(111) Si(311) Si(111) Smallest Focus H x V [µm 2] 30 x 20 4 x 1 200 x 60 Divergence H x V [mrad 2] 0. 2 x 0. 15 0. 5 x 0. 3 0. 04 x 0. 01 Demagnification H/V 1: 12/1: 15 1: 40/1: 30 1: 1. 4 / 1: 1. 2 Intensity [ph/sec], Si 111 10123*1013 Both MX 1 and MX 2 will be equipped with Mini. Kappa device 20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup

First light at MX 2 – last Friday 28/09/2009 Gleb Bourenkov Meeting Kappa Workgroup First light at MX 2 – last Friday 28/09/2009 Gleb Bourenkov Meeting Kappa Workgroup

PETRAIII MX – BW 7 A DORIS test bench 20/09/2010 Gleb Bourenkov Meeting Kappa PETRAIII MX – BW 7 A DORIS test bench 20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup

Ø MD 2/Mini. Kappa recived in 07 -10/2009 Ø commissioned at BW 7 A/DORIS Ø MD 2/Mini. Kappa recived in 07 -10/2009 Ø commissioned at BW 7 A/DORIS beamline STAC with TINE interface 20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup

MD 3 – Kappa diffractometer for microcrystallography, SOC in 100 nm range Florent Cipriani MD 3 – Kappa diffractometer for microcrystallography, SOC in 100 nm range Florent Cipriani and Frank Felicaz 20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup

MARVIN sample changer MD 2/MD 3 diffractometer MARVIN Focusing KB mirrors BCU Prototype at MARVIN sample changer MD 2/MD 3 diffractometer MARVIN Focusing KB mirrors BCU Prototype at DORIS beamline BW 7 b. In operation for in house users. 20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup

MX data collection software Mx. Cu. BE GUI Scripting Python – Py. TINE Shell MX data collection software Mx. Cu. BE GUI Scripting Python – Py. TINE Shell – TINE CS Data Collection Server Detector Server 20/09/2010 Gleb Bourenkov MD 2 Server Detector stage Ener gy Attr Ring current … [email protected] SAB Meeting

20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup 20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup

20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup 20/09/2010 Gleb Bourenkov Meeting Kappa Workgroup

MD 2 linear positioning repeatability • Gauge resolution 0. 1 µm • Spindle alignment MD 2 linear positioning repeatability • Gauge resolution 0. 1 µm • Spindle alignment table 0. 1(3) µm r. m. s. • Centering table 0. 2 µm r. m. s. • Aperture etc. 0. 2 µm r. m. s. ΩY 25 20 15 10 5 -0. 4 20/09/2010 Gleb Bourenkov -0. 2 0. 4 [email protected] SAB Meeting

Sphere of Confusion: measurements position vs anlgle 0. 033 µm/pixel Fourier spectrum 1 st Sphere of Confusion: measurements position vs anlgle 0. 033 µm/pixel Fourier spectrum 1 st harmonic - centering 22 2 3 continuous rotation, fast, vertical steps, OAV 0. 33 µm/pixel (LR) 0. 033 µm/pixel continuous, fast, horizontal continuous, slow, horizontal steps, OAV, offset steps, OAV, slow, mini. Kappa, open steps, OAV, slow, mini. Kappa, closed 20/09/2010 Gleb Bourenkov [email protected] SAB Meeting 23

MD 2 SOC without mini. Kappa 0. 9 µm r. m. s. = 0. MD 2 SOC without mini. Kappa 0. 9 µm r. m. s. = 0. 25 µm peak-to-peak diameter = 0. 9 µm 0. 75 µm 2 nd+3 rd harmonics gravity effects on centering table 0. 3 µm 20 th+23 rd harmonics Omega motor poles 20/09/2010 Gleb Bourenkov [email protected] SAB Meeting

SOC with mini. Kappa miniκ=60 miniκ=0 constant magnet SOC with mini. Kappa: 0. 7 SOC with mini. Kappa miniκ=60 miniκ=0 constant magnet SOC with mini. Kappa: 0. 7 µm r. m. s. 2. 4 µm peak-to-peak diameter only the 2 nd harmonic (centering table) amplitude increase, no phase change, no new features 20/09/2010 Gleb Bourenkov [email protected] SAB Meeting

Mini. Kappa: repeatability move to reference, move to position CONFUSION! re-initialize move around, come Mini. Kappa: repeatability move to reference, move to position CONFUSION! re-initialize move around, come back off by ~3º back within <0. 05º When motors are driven from the MD 2 Kappa motor phi tuning box using default “motor” coordinate system, the backlash and relaxation corrections are not applied. (Positioning is not repeatable) When driven from the device server or in any other way using the “device” coordinate system the corrections are applied, but the position is not updated during the backlash correction – so it looks like it is not applied. kappa (Positioning is repeatable) Device is OK, control via STAC is OK 24/11/2009 Gleb Bourenkov Meeting Bilateral GR-HH Instrumentation